Directed Electronics G4203P Bedienungsanleitung

Agilent TechnologiesAgilent 1260 Infinity Bio-inert Quaternary PumpUser Manual

10 Bio-inert Quaternary Pump User Manual1 IntroductionIntroduction to the PumpIntroduction to the PumpThe bio-inert quaternary pump comprises an optio

100 Bio-inert Quaternary Pump User Manual8 Test Functions and CalibrationSystem Pressure TestIf the test fails again, insert the blank nut at the outl

Bio-inert Quaternary Pump User Manual 101Test Functions and Calibration8System Pressure TestSystem Pressure Test failedThe test will fail, if the sum

102 Bio-inert Quaternary Pump User Manual8 Test Functions and CalibrationLeak Rate TestLeak Rate TestIntroductionThe Leak Rate Test is used for verify

Bio-inert Quaternary Pump User Manual 103Test Functions and Calibration8Leak Rate TestInitially, the pressure is increased to about 100 bar below the

104 Bio-inert Quaternary Pump User Manual8 Test Functions and CalibrationLeak Rate TestRunning the TestRunning the test from the Agilent Lab Advisor1

Bio-inert Quaternary Pump User Manual 105Test Functions and Calibration8Leak Rate TestPotential Causes of Leak Rate Test FailureSecondary LeakIf a lea

106 Bio-inert Quaternary Pump User Manual8 Test Functions and CalibrationLeak Rate Test

107Bio-inert Quaternary Pump User ManualAgilent Technologies9MaintenanceIntroduction to Maintenance 108Warnings and Cautions 109Overview of Maintenanc

108 Bio-inert Quaternary Pump User Manual9 MaintenanceIntroduction to MaintenanceIntroduction to MaintenanceThe module is designed for easy repair. Th

Bio-inert Quaternary Pump User Manual 109Maintenance9Warnings and CautionsWarnings and CautionsWARNINGToxic, flammable and hazardous solvents, samples

Bio-inert Quaternary Pump User Manual 11Introduction1Overview of the Hydraulic PathOverview of the Hydraulic PathThe bio-inert quaternary pump is base

110 Bio-inert Quaternary Pump User Manual9 MaintenanceWarnings and CautionsCAUTIONSafety standards for external equipment➔ If you connect external equ

Bio-inert Quaternary Pump User Manual 111Maintenance9Overview of MaintenanceOverview of MaintenanceThe following pages describe maintenance (simple re

112 Bio-inert Quaternary Pump User Manual9 MaintenanceCleaning the ModuleCleaning the ModuleThe module case should be kept clean. Cleaning should be d

Bio-inert Quaternary Pump User Manual 113Maintenance9Checking and Replacing the Solvent FilterChecking and Replacing the Solvent FilterA functional so

114 Bio-inert Quaternary Pump User Manual9 MaintenanceExchanging the Active Inlet Valve (AIV) or its CartridgeExchanging the Active Inlet Valve (AIV)

Bio-inert Quaternary Pump User Manual 115Maintenance9Exchanging the Active Inlet Valve (AIV) or its Cartridge5 Using a 14 mm wrench loosen the active

116 Bio-inert Quaternary Pump User Manual9 MaintenanceExchanging the Active Inlet Valve (AIV) or its Cartridge13 Reconnect the solvent inlet tube to t

Bio-inert Quaternary Pump User Manual 117Maintenance9Exchanging the Outlet ValveExchanging the Outlet ValveWhen If internally leakingTools required p/

118 Bio-inert Quaternary Pump User Manual9 MaintenanceExchanging the Outlet Valve1Using the 1/4 inch wrench disconnect the valve capillary from the ou

Bio-inert Quaternary Pump User Manual 119Maintenance9Exchanging the Purge Valve Frit or the Purge ValveExchanging the Purge Valve Frit or the Purge Va

12 Bio-inert Quaternary Pump User Manual1 IntroductionOverview of the Hydraulic PathHydraulic PathFigure 2 Hydraulic Path of the Bio-inert Quaternary

120 Bio-inert Quaternary Pump User Manual9 MaintenanceExchanging the Purge Valve Frit or the Purge Valve1Using a 1/4 inch wrench disconnect the pump o

Bio-inert Quaternary Pump User Manual 121Maintenance9Exchanging the Purge Valve Frit or the Purge Valve5Place a new frit into the purge valve with the

122 Bio-inert Quaternary Pump User Manual9 MaintenanceRemoving the Pump Head AssemblyRemoving the Pump Head AssemblyWhen • Exchanging the seals• Excha

Bio-inert Quaternary Pump User Manual 123Maintenance9Removing the Pump Head Assembly1Remove the front cover by pressing the clip fasteners on both sid

124 Bio-inert Quaternary Pump User Manual9 MaintenanceRemoving the Pump Head Assembly6Using a 4 mm hexagonal key, stepwise loosen the two pump head sc

Bio-inert Quaternary Pump User Manual 125Maintenance9Seal Wear-in ProcedureSeal Wear-in Procedure1 Place a bottle with 100 mL of isopropanol in the so

126 Bio-inert Quaternary Pump User Manual9 MaintenanceMaintenance of the Pump HeadMaintenance of the Pump HeadWhen When maintaining seal wash optionTo

Bio-inert Quaternary Pump User Manual 127Maintenance9Maintenance of the Pump Head1Remove the seal holder and the seal wash support rings from the pist

128 Bio-inert Quaternary Pump User Manual9 MaintenanceMaintenance of the Pump Head5Place a seal wash gasket in the recess of the support ring. Put the

Bio-inert Quaternary Pump User Manual 129Maintenance9Reinstalling the Pump Head AssemblyReinstalling the Pump Head AssemblyWhen When reassembling the

Bio-inert Quaternary Pump User Manual 13Introduction1Overview of the Hydraulic PathFigure 3 Hydraulic Path of the Quaternary PumpHow Does the Pump Wor

130 Bio-inert Quaternary Pump User Manual9 MaintenanceReinstalling the Pump Head Assembly3Reconnect all capillaries, tubes and (if installed) the acti

Bio-inert Quaternary Pump User Manual 131Maintenance9Exchanging the Multi-Channel Gradient Valve (MCGV)Exchanging the Multi-Channel Gradient Valve (MC

132 Bio-inert Quaternary Pump User Manual9 MaintenanceExchanging the Multi-Channel Gradient Valve (MCGV)1Disconnect the connecting tube, waste tube an

Bio-inert Quaternary Pump User Manual 133Maintenance9Exchanging the Multi-Channel Gradient Valve (MCGV)4Place the new MCGV into position. Make sure th

134 Bio-inert Quaternary Pump User Manual9 MaintenanceExchanging the Optional Interface BoardExchanging the Optional Interface BoardWhen Board defecti

Bio-inert Quaternary Pump User Manual 135Maintenance9Exchanging the Optional Interface Board1 Switch off the pump at the main power switch, unplug the

136 Bio-inert Quaternary Pump User Manual9 MaintenanceReplacing the Module’s FirmwareReplacing the Module’s FirmwareTo upgrade/downgrade the module’s

137Bio-inert Quaternary Pump User ManualAgilent Technologies10Parts for MaintenancePump Head Assembly with Seal Wash Option 138Outlet Valve 140Purge V

138 Bio-inert Quaternary Pump User Manual10 Parts for MaintenancePump Head Assembly with Seal Wash OptionPump Head Assembly with Seal Wash OptionFor b

Bio-inert Quaternary Pump User Manual 139Parts for Maintenance10Pump Head Assembly with Seal Wash OptionFigure 11 Pump Head with Seal Wash Option&

14 Bio-inert Quaternary Pump User Manual1 IntroductionOverview of the Hydraulic Pathdepending on the flow rate. The microprocessor controls all flow r

140 Bio-inert Quaternary Pump User Manual10 Parts for MaintenanceOutlet ValveOutlet Valve Figure 12 Outlet valve, bio-inertFor bio-inert modules use b

Bio-inert Quaternary Pump User Manual 141Parts for Maintenance10Purge Valve AssemblyPurge Valve AssemblyFigure 13 Purge valve assembly, bio-inertFor b

142 Bio-inert Quaternary Pump User Manual10 Parts for MaintenanceActive Inlet ValveActive Inlet ValveFor bio-inert modules use bio-inert parts only!p/

Bio-inert Quaternary Pump User Manual 143Parts for Maintenance10Active Inlet ValveFigure 14 Active inlet valve

144 Bio-inert Quaternary Pump User Manual10 Parts for MaintenanceAccessory Kit, Bio-inert (G5611-68755)Accessory Kit, Bio-inert (G5611-68755)Accessory

Bio-inert Quaternary Pump User Manual 145Parts for Maintenance10Starter-Kit Bio-inertStarter-Kit Bio-inertStarter-Kit Bio-inert HPLC (p/n G5611-68707

146 Bio-inert Quaternary Pump User Manual10 Parts for MaintenanceSolvent CabinetSolvent CabinetItem p/n Description1 5065-9981 Solvent cabinet, includ

Bio-inert Quaternary Pump User Manual 147Parts for Maintenance10Solvent CabinetFigure 15 Solvent Cabinet Parts,*$+

148 Bio-inert Quaternary Pump User Manual10 Parts for MaintenanceBottle Head AssemblyBottle Head AssemblyFigure 16 Bottle-Head Assembly PartsItem p/n

Bio-inert Quaternary Pump User Manual 149Parts for Maintenance10Hydraulic PathHydraulic PathFor bio-inert modules use bio-inert parts only!Item p/n De

Bio-inert Quaternary Pump User Manual 15Introduction1Overview of the Hydraulic PathWhen turned on, the pump runs through an initialization procedure t

150 Bio-inert Quaternary Pump User Manual10 Parts for MaintenanceHydraulic PathFigure 17 Hydraulic Flow Path&'()*+

Bio-inert Quaternary Pump User Manual 151Parts for Maintenance10System Tool KitSystem Tool KitHPLC System Tool Kit (p/n G4203-68708)p/n Description01

152 Bio-inert Quaternary Pump User Manual10 Parts for MaintenancePreventive Maintenance KitPreventive Maintenance KitFor bio-inert modules use bio-ine

153Bio-inert Quaternary Pump User ManualAgilent Technologies11Identifying CablesCable Overview 154Analog Cables 156Remote Cables 158BCD Cables 161CAN/

154 Bio-inert Quaternary Pump User Manual11 Identifying CablesCable OverviewCable OverviewAnalog cablesRemote cablesBCD cablesNOTENever use cables oth

Bio-inert Quaternary Pump User Manual 155Identifying Cables11Cable OverviewCAN cablesLAN cablesExternal Contact CableRS-232 cablesp/n Description5181-

156 Bio-inert Quaternary Pump User Manual11 Identifying CablesAnalog CablesAnalog CablesOne end of these cables provides a BNC connector to be connect

Bio-inert Quaternary Pump User Manual 157Identifying Cables11Analog CablesAgilent Module to General Purposep/n 01046-60105 Pin Pin Agilent moduleSigna

158 Bio-inert Quaternary Pump User Manual11 Identifying CablesRemote CablesRemote CablesOne end of these cables provides a Agilent Technologies APG (A

Bio-inert Quaternary Pump User Manual 159Identifying Cables11Remote CablesAgilent Module to 3396 Series III / 3395B IntegratorsAgilent Module to Agile

16 Bio-inert Quaternary Pump User Manual1 IntroductionOverview of the Hydraulic PathWith a compressibility value set the processor calculates a compen

160 Bio-inert Quaternary Pump User Manual11 Identifying CablesRemote CablesAgilent Module to General Purposep/n 01046-60201 Pin Universal Pin Agilent

Bio-inert Quaternary Pump User Manual 161Identifying Cables11BCD CablesBCD CablesOne end of these cables provides a 15-pin BCD connector to be connect

162 Bio-inert Quaternary Pump User Manual11 Identifying CablesBCD CablesAgilent Module to 3396 Integratorsp/n 03396-60560 Pin 3396 Pin Agilent moduleS

Bio-inert Quaternary Pump User Manual 163Identifying Cables11CAN/LAN CablesCAN/LAN CablesBoth ends of this cable provide a modular plug to be connecte

164 Bio-inert Quaternary Pump User Manual11 Identifying CablesExternal Contact CableExternal Contact CableOne end of this cable provides a 15-pin plug

Bio-inert Quaternary Pump User Manual 165Identifying Cables11Agilent Module to PCAgilent Module to PCp/n DescriptionG1530-60600 RS-232 cable, 2 mRS232

166 Bio-inert Quaternary Pump User Manual11 Identifying CablesAgilent 1200 Module to PrinterAgilent 1200 Module to Printerp/n Description5181-1529 Cab

167Bio-inert Quaternary Pump User ManualAgilent Technologies12Hardware InformationElectrical Connections 168Rear View of the Module 169Interfaces 170O

168 Bio-inert Quaternary Pump User Manual12 Hardware InformationElectrical ConnectionsElectrical Connections• The CAN bus is a serial bus with high sp

Bio-inert Quaternary Pump User Manual 169Hardware Information12Electrical ConnectionsRear View of the ModuleFigure 18 Rear view of the pump

Bio-inert Quaternary Pump User Manual 17Introduction1Bio-inert MaterialsBio-inert MaterialsFor the Agilent 1260 Infinity Bio-inert LC system, Agilent

170 Bio-inert Quaternary Pump User Manual12 Hardware InformationInterfacesInterfacesThe Agilent 1200 Infinity Series modules provide the following int

Bio-inert Quaternary Pump User Manual 171Hardware Information12InterfacesDetectorsG1314B VWD VLG1314C VWD VL+2 Yes No Yes 1 YesG1314E/F VWD 2 No Yes Y

172 Bio-inert Quaternary Pump User Manual12 Hardware InformationInterfaces• CAN connectors as interface to other modules• LAN connector as interface t

Bio-inert Quaternary Pump User Manual 173Hardware Information12InterfacesThe RS-232C is designed as DCE (data communication equipment) with a 9-pin ma

174 Bio-inert Quaternary Pump User Manual12 Hardware InformationInterfacesFigure 19 RS-232 CableAnalog Signal OutputThe analog signal output can be di

Bio-inert Quaternary Pump User Manual 175Hardware Information12Interfaces• standard TTL levels (0 V is logic true, + 5.0 V is false),• fan-out is 10,•

176 Bio-inert Quaternary Pump User Manual12 Hardware InformationSetting the 8-bit Configuration Switch (without On-board) LANSetting the 8-bit Configu

Bio-inert Quaternary Pump User Manual 177Hardware Information12Setting the 8-bit Configuration Switch (without On-board) LANCommunication Settings for

178 Bio-inert Quaternary Pump User Manual12 Hardware InformationSetting the 8-bit Configuration Switch (without On-board) LANOne start bit and one sto

Bio-inert Quaternary Pump User Manual 179Hardware Information12Setting the 8-bit Configuration Switch (without On-board) LANSpecial SettingsThe specia

18 Bio-inert Quaternary Pump User Manual1 IntroductionBio-inert MaterialsFor ensuring optimum bio-compatibility of your Agilent 1260 Infinity Bio-iner

180 Bio-inert Quaternary Pump User Manual12 Hardware InformationSetting the 8-bit Configuration Switch (without On-board) LAN

181Bio-inert Quaternary Pump User ManualAgilent Technologies13AppendixGeneral Safety Information 182The Waste Electrical and Electronic Equipment Dire

182 Bio-inert Quaternary Pump User Manual13 AppendixGeneral Safety InformationGeneral Safety InformationGeneral Safety Information The following gener

Bio-inert Quaternary Pump User Manual 183Appendix13General Safety Informationthe instrument must be made inoperative and be secured against any intend

184 Bio-inert Quaternary Pump User Manual13 AppendixGeneral Safety InformationSafety SymbolsTab le 19 Safety SymbolsSymbol DescriptionThe apparatus is

Bio-inert Quaternary Pump User Manual 185Appendix13The Waste Electrical and Electronic Equipment DirectiveThe Waste Electrical and Electronic Equipmen

186 Bio-inert Quaternary Pump User Manual13 AppendixBatteries InformationBatteries InformationWARNINGLithium batteries may not be disposed-off into th

Bio-inert Quaternary Pump User Manual 187Appendix13Radio InterferenceRadio InterferenceCables supplied by Agilent Technologies are screened to provide

188 Bio-inert Quaternary Pump User ManualSound EmissionSound EmissionManufacturer’s DeclarationThis statement is provided to comply with the requireme

Bio-inert Quaternary Pump User Manual 189Agilent Technologies on InternetAgilent Technologies on InternetFor the latest information on products and se

Bio-inert Quaternary Pump User Manual 19Introduction1Early Maintenance FeedbackEarly Maintenance FeedbackMaintenance requires the exchange of componen

190 Bio-inert Quaternary Pump User ManualIndexIndex88-bit configuration switchwithout On-Board LAN 176Aaccessory kit 29, 144active inlet valve cartri

Bio-inert Quaternary Pump User Manual 191Indexerror messagespump error 80error messagescompensation sensor open 78compensation sensor short 78encoder

192 Bio-inert Quaternary Pump User ManualIndexNnon-operating altitude 25non-operating temperature 25Ooperating Altitude 25operating temperature 25oper

Bio-inert Quaternary Pump User Manual 193Indexsystem pressure test, evaluating results 99system pressure test 65, 97running the test 99system setup a

Agilent Technologies 2011-2012Printed in Germany 05/12*G5611-90000**G5611-90000*G5611-90000 Rev. Cwww.agilent.comAgilent TechnologiesIn This BookThi

Bio-inert Quaternary Pump User ManualNotices© Agilent Technologies, Inc. 2011-2012No part of this manual may be reproduced in any form or by any means

20 Bio-inert Quaternary Pump User Manual1 IntroductionInstrument LayoutInstrument LayoutThe industrial design of the module incorporates several innov

21Bio-inert Quaternary Pump User ManualAgilent Technologies2Site Requirements and SpecificationsSite Requirements 22Physical Specifications 25Performa

22 Bio-inert Quaternary Pump User Manual2 Site Requirements and SpecificationsSite RequirementsSite RequirementsA suitable environment is important to

Bio-inert Quaternary Pump User Manual 23Site Requirements and Specifications2Site RequirementsPower CordsDifferent power cords are offered as options

24 Bio-inert Quaternary Pump User Manual2 Site Requirements and SpecificationsSite RequirementsBench SpaceThe module dimensions and weight (see Table

Bio-inert Quaternary Pump User Manual 25Site Requirements and Specifications2Physical SpecificationsPhysical SpecificationsTab le 2 Physical Specifica

26 Bio-inert Quaternary Pump User Manual2 Site Requirements and SpecificationsPerformance SpecificationsPerformance SpecificationsTab le 3 Specificati

27Bio-inert Quaternary Pump User ManualAgilent Technologies3Installing the PumpUnpacking the Pump 28Delivery Checklist 28Accessory Kit 29Optimizing th

28 Bio-inert Quaternary Pump User Manual3 Installing the PumpUnpacking the PumpUnpacking the PumpIf the delivery packaging shows signs of external dam

Bio-inert Quaternary Pump User Manual 29Installing the Pump3Unpacking the PumpAccessory KitAccessory Kit (Bio-inert) (p/n G5611-68755)699975-902 Colu

Bio-inert Quaternary Pump User Manual 3In This Guide...In This Guide...This manual covers the Agilent 1260 Infinity Bio-inert Quaternary Pump G5611A.1

30 Bio-inert Quaternary Pump User Manual3 Installing the PumpOptimizing the Stack ConfigurationOptimizing the Stack ConfigurationIf your module is par

Bio-inert Quaternary Pump User Manual 31Installing the Pump3Optimizing the Stack ConfigurationFigure 5 Recommended Stack Configuration (Front View)Hda

32 Bio-inert Quaternary Pump User Manual3 Installing the PumpOptimizing the Stack ConfigurationFigure 6 Recommended Stack Configuration (Rear View)A6C

Bio-inert Quaternary Pump User Manual 33Installing the Pump3Installing the PumpInstalling the PumpFor other cables see text below and “Cable Overview”

34 Bio-inert Quaternary Pump User Manual3 Installing the PumpInstalling the Pump1 Place the module on the bench in a horizontal position.2 Ensure the

Bio-inert Quaternary Pump User Manual 35Installing the Pump3Installing the Pump4 Connect the required interface cables to the quaternary pump, see “Co

36 Bio-inert Quaternary Pump User Manual3 Installing the PumpConnecting Modules and Control SoftwareConnecting Modules and Control SoftwareConnecting

Bio-inert Quaternary Pump User Manual 37Installing the Pump3Connecting Modules and Control SoftwareConnecting Control Software and/or G4208 A Instant

38 Bio-inert Quaternary Pump User Manual3 Installing the PumpFlow Connections of the PumpFlow Connections of the Pump Parts required # Description1 Ot

Bio-inert Quaternary Pump User Manual 39Installing the Pump3Flow Connections of the Pump1 Remove the front cover by pressing the snap fasteners on bot

4 Bio-inert Quaternary Pump User ManualIn This Guide...8 Test Functions and CalibrationThis chapter describes the tests for the module.9 MaintenanceTh

40 Bio-inert Quaternary Pump User Manual3 Installing the PumpFlow Connections of the Pump9 Prime your system before first use (see “Initial Priming” o

Bio-inert Quaternary Pump User Manual 41Installing the Pump3Priming the SystemPriming the SystemInitial Priming When Before a new degasser or new solv

42 Bio-inert Quaternary Pump User Manual3 Installing the PumpPriming the System1 Open the purge valve of the pump2 Set the flow rate to 5 mL/min.3 Sel

Bio-inert Quaternary Pump User Manual 43Installing the Pump3Priming the SystemRegular Priming1 Open the purge valve of your pump by turning it counter

44 Bio-inert Quaternary Pump User Manual3 Installing the PumpPriming the SystemChanging Solvents1 If the channel is not filled with buffer, proceed to

Bio-inert Quaternary Pump User Manual 45Installing the Pump3Priming the SystemTab le 4 Choice of Priming Solvents for Different PurposesActivity Solve

46 Bio-inert Quaternary Pump User Manual3 Installing the PumpPriming the System

47Bio-inert Quaternary Pump User ManualAgilent Technologies4Using the PumpHints for Successful Use of the Quaternary Pump 48Prevent Blocking of Solven

48 Bio-inert Quaternary Pump User Manual4 Using the PumpHints for Successful Use of the Quaternary PumpHints for Successful Use of the Quaternary Pump

Bio-inert Quaternary Pump User Manual 49Using the Pump4Prevent Blocking of Solvent FiltersPrevent Blocking of Solvent FiltersContaminated solvents or

Bio-inert Quaternary Pump User Manual 5ContentsContents1 Introduction 9Introduction to the Pump 10Overview of the Hydraulic Path 11Bio-inert Materials

50 Bio-inert Quaternary Pump User Manual4 Using the PumpAlgae Growth in HPLC SystemsAlgae Growth in HPLC SystemsThe presence of algae in HPLC systems

Bio-inert Quaternary Pump User Manual 51Using the Pump4Solvent InformationSolvent InformationSolvent InformationObserve the following recommendations

52 Bio-inert Quaternary Pump User Manual4 Using the PumpSolvent InformationPEEKPEEK (Polyether-Ether Ketones) combines excellent properties regarding

Bio-inert Quaternary Pump User Manual 53Using the Pump4Solvent InformationGoldGold is inert against all common HPLC solvents, acids and bases within t

54 Bio-inert Quaternary Pump User Manual4 Using the PumpSolvent Information

55Bio-inert Quaternary Pump User ManualAgilent Technologies5Optimizing PerformanceWhen to Use a Degasser 56Operational Hints for the Multi Channel Gra

56 Bio-inert Quaternary Pump User Manual5 Optimizing PerformanceWhen to Use a DegasserWhen to Use a DegasserThe bio-inert quaternary pump has a built-

Bio-inert Quaternary Pump User Manual 57Optimizing Performance5Operational Hints for the Multi Channel Gradient Valve (MCGV)Operational Hints for the

58 Bio-inert Quaternary Pump User Manual5 Optimizing PerformanceWhen to use the Seal Wash OptionWhen to use the Seal Wash OptionHighly concentrated bu

Bio-inert Quaternary Pump User Manual 59Optimizing Performance5Choosing the Right Pump SealsChoosing the Right Pump SealsThe standard seal for the pum

6 Bio-inert Quaternary Pump User ManualContents6 Troubleshooting and Diagnostics 63Overview of the Module’s Indicators and Test Functions 64Status Ind

60 Bio-inert Quaternary Pump User Manual5 Optimizing PerformanceOptimize the Compressibility Compensation SettingOptimize the Compressibility Compensa

Bio-inert Quaternary Pump User Manual 61Optimizing Performance5Optimize the Compressibility Compensation SettingTab le 5 Solvent Compressibility Solve

62 Bio-inert Quaternary Pump User Manual5 Optimizing PerformanceOptimize the Compressibility Compensation Setting

63Bio-inert Quaternary Pump User ManualAgilent Technologies6Troubleshooting and DiagnosticsOverview of the Module’s Indicators and Test Functions 64St

64 Bio-inert Quaternary Pump User Manual6 Troubleshooting and DiagnosticsOverview of the Module’s Indicators and Test FunctionsOverview of the Module’

Bio-inert Quaternary Pump User Manual 65Troubleshooting and Diagnostics6Overview of the Module’s Indicators and Test FunctionsSystem Pressure TestThe

66 Bio-inert Quaternary Pump User Manual6 Troubleshooting and DiagnosticsStatus IndicatorsStatus IndicatorsTwo status indicators are located on the fr

Bio-inert Quaternary Pump User Manual 67Troubleshooting and Diagnostics6Status IndicatorsModule Status IndicatorThe module status indicator indicates

68 Bio-inert Quaternary Pump User Manual6 Troubleshooting and DiagnosticsUser InterfacesUser InterfacesDepending on the user interface, the available

Bio-inert Quaternary Pump User Manual 69Troubleshooting and Diagnostics6Agilent Lab Advisor SoftwareAgilent Lab Advisor SoftwareThe Agilent Lab Adviso

Bio-inert Quaternary Pump User Manual 7Contents10 Parts for Maintenance 137Pump Head Assembly with Seal Wash Option 138Outlet Valve 140Purge Valve Ass

70 Bio-inert Quaternary Pump User Manual6 Troubleshooting and DiagnosticsAgilent Lab Advisor Software

71Bio-inert Quaternary Pump User ManualAgilent Technologies7Error InformationWhat Are Error Messages 73General Error Messages 74Timeout 74Shut-Down 74

72 Bio-inert Quaternary Pump User Manual7 Error InformationAgilent Lab Advisor SoftwareTemperature Limit Exceeded 88Servo Restart Failed 89Pump Head M

Bio-inert Quaternary Pump User Manual 73Error Information7What Are Error MessagesWhat Are Error MessagesError messages are displayed in the user inter

74 Bio-inert Quaternary Pump User Manual7 Error InformationGeneral Error MessagesGeneral Error MessagesGeneral error messages are generic to all Agile

Bio-inert Quaternary Pump User Manual 75Error Information7General Error MessagesRemote TimeoutA not-ready condition is still present on the remote inp

76 Bio-inert Quaternary Pump User Manual7 Error InformationGeneral Error MessagesSynchronization LostDuring an analysis, the internal synchronization

Bio-inert Quaternary Pump User Manual 77Error Information7General Error MessagesLeak Sensor Open The leak sensor in the module has failed (open circui

78 Bio-inert Quaternary Pump User Manual7 Error InformationGeneral Error MessagesCompensation Sensor OpenThe ambient-compensation sensor (NTC) on the

Bio-inert Quaternary Pump User Manual 79Error Information7General Error MessagesFan FailedThe cooling fan in the module has failed. The hall sensor on

8 Bio-inert Quaternary Pump User ManualContents

80 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesModule Error MessagesThese errors are pump specific.Restart Without Co

Bio-inert Quaternary Pump User Manual 81Error Information7Module Error MessagesPressure Above Upper LimitThe system pressure has exceeded the upper pr

82 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesPressure Below Lower LimitThe system pressure has fallen below the low

Bio-inert Quaternary Pump User Manual 83Error Information7Module Error MessagesMissing Pressure ReadingThe pressure readings read by the pump ADC (ana

84 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesValve FuseValve Fuse 0: Channels A and BValve Fuse 1: Channels C and D

Bio-inert Quaternary Pump User Manual 85Error Information7Module Error MessagesValve Failed (MCGV/SSV)Valve 0 Failed: valve AValve 1 Failed: valve BVa

86 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesMotor-Drive PowerThe current drawn by the pump motor exceeded the maxi

Bio-inert Quaternary Pump User Manual 87Error Information7Module Error MessagesEncoder MissingThe optical encoder on the pump motor in the module is m

88 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesTemperature Out of RangeThe temperature sensor readings in the motor-d

Bio-inert Quaternary Pump User Manual 89Error Information7Module Error MessagesServo Restart FailedThe pump motor in the module was unable to move int

9Bio-inert Quaternary Pump User ManualAgilent Technologies1IntroductionIntroduction to the Pump 10Overview of the Hydraulic Path 11Hydraulic Path 12Ho

90 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesIndex LimitThe time required by the piston to reach the encoder index

Bio-inert Quaternary Pump User Manual 91Error Information7Module Error MessagesIndex MissingThe encoder index position in the module was not found dur

92 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesInitialization FailedThe module failed to initialize successfully with

Bio-inert Quaternary Pump User Manual 93Error Information7Module Error MessagesWait TimeoutWhen running certain tests in the diagnostics mode or other

94 Bio-inert Quaternary Pump User Manual7 Error InformationModule Error MessagesDegasser: cannot read signalThe pump board gets no or wrong pressure s

95Bio-inert Quaternary Pump User ManualAgilent Technologies8Test Functions and CalibrationIntroduction 96System Pressure Test 97Running the Test 99Eva

96 Bio-inert Quaternary Pump User Manual8 Test Functions and CalibrationIntroductionIntroductionAll tests are described based on the Agilent Lab Advis

Bio-inert Quaternary Pump User Manual 97Test Functions and Calibration8System Pressure TestSystem Pressure TestIntroductionThe System Pressure Test is

98 Bio-inert Quaternary Pump User Manual8 Test Functions and CalibrationSystem Pressure TestIn the first phase of the test, the pump delivers flow at

Bio-inert Quaternary Pump User Manual 99Test Functions and Calibration8System Pressure TestRunning the TestRunning the test from the Agilent Lab Advis